浩瀚色谱（山东）应用技术开发有限公司研发一种氢、氘化氢和氘氢同位素定量检测的方法，该方法是以氖气作为载气，气相色谱仪采用了双柱双温系统，选择50℃进样温度，通过注射器或气体进样阀进样，进样量为0.1－2.2mL，样品气经气相色谱柱分离后的气体通过检测器产生电信号，经前置放大器将信号放大后，由色谱工作站记录色谱峰氢气、氘化氢、氘气的峰面积，采用体积校正因子归一化法或外标法测定氢(H2)、氘化氢(HD)和氘(D2)含量，得到检测结果。特点是：氢同位素的分离效果好，检测灵敏度高，氘气纯度的检测可达99.99％以上，大剂量进样氘化氢(HD)和氘(D2)，其峰不重叠，从而保证了高纯氘气的定量检测，检测中不用配制标准气，简化了操作过程，便于氘气生产过程中的在线检测。
名称：填充柱
规格：1m*2mm
型号：MnCL2/γ-Al2O3
应用：低丰度的氢同位素检测
Haohan Chromatography (Shandong) Applied Technology Development Co., Ltd. has developed a method for quantitative detection of hydrogen, hydrogen deuteride and deuterium hydrogen isotopes. The method uses neon as the carrier gas, and the gas chromatograph adopts a dual-column dual-temperature system. Select 50 The sample temperature is ℃, and the sample is injected through a syringe or a gas injection valve. The sample volume is 0.1-2.2mL. The gas separated by the sample gas by the gas chromatographic column generates an electrical signal through the detector. After the signal is amplified by the preamplifier, The chromatographic workstation records the peak areas of chromatographic peak hydrogen, hydrogen deuteride, and deuterium gas, and uses volume correction factor normalization method or external standard method to determine the content of hydrogen (H2), hydrogen deuteride (HD) and deuterium (D2) to obtain Test results. The characteristics are: the separation effect of hydrogen isotopes is good, the detection sensitivity is high, the detection of deuterium gas purity can reach more than 99.99%, and the high-dose injection of deuterated hydrogen (HD) and deuterium (D2), the peaks do not overlap, thus ensuring high For the quantitative detection of pure deuterium gas, there is no need to prepare standard gas in the detection, which simplifies the operation process and facilitates online detection in the production process of deuterium gas.
Name: Packed column
Specification: 2m3mm
Model: MnCL2/γ-Al2O3
Application: Low-abundance hydrogen isotope detection
